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A new synthesis method of flexible microcapsules applied for electrophoresis display
Dai, Lu1,2; Li, Peidong1,2; Tu, Qiang2; Sun, Maojun3; Yuan, Jiahu1,2; Cui, Yuehua1,2
2024-06-21
摘要This study prepared a new type of electrophoretic display microcapsule with flexibility and strength, namely gum arabic/gelatin/urea-formaldehyde resin microcapsule, based on polysaccharides as the reaction starting point, combined with proteins and resins. The composition, morphology and thermal stability of the microcapsules were tested by Fourier transform infrared spectroscopy, stereo fluorescence microscopy, scanning electron microscopy and thermogravimetric analysis. It was found that the morphology and stability of the new microcapsules prepared by the method are better than those prepared by the traditional complex coacervation method or the in-situ polymerization method. At the same time, it showed that the rotational speed was between 1000 rpm and 1200 rpm, the concentrations of gum arabic and gelatin were 3 wt%, the reaction pH between 3 and 3.5, the reaction duration is between 150 min and 180 min, the ammonium chloride was 20 wt%, and resorcinol was 6 wt%, the reaction between the urea-formaldehyde prepolymer and the electro-neutralizer formed by gelatin and gum arabic was sufficient, the microcapsule wall structure was uniform and consistent, with a dense resin based structure on the outer layer and a flexible blend structure inside.
关键词Gum acacia and gelatin Urea -formaldehyde resin Electrophoresis display microcapsule
DOI10.1016/j.polymer.2024.127205
发表期刊POLYMER
ISSN0032-3861
卷号306页码:11
通讯作者Cui, Yuehua(yhcui@cigit.ac.cn)
收录类别SCI
WOS记录号WOS:001250038400002
语种英语