KMS Chongqing Institute of Green and Intelligent Technology, CAS
A new synthesis method of flexible microcapsules applied for electrophoresis display | |
Dai, Lu1,2; Li, Peidong1,2; Tu, Qiang2; Sun, Maojun3; Yuan, Jiahu1,2![]() ![]() ![]() | |
2024-06-21 | |
摘要 | This study prepared a new type of electrophoretic display microcapsule with flexibility and strength, namely gum arabic/gelatin/urea-formaldehyde resin microcapsule, based on polysaccharides as the reaction starting point, combined with proteins and resins. The composition, morphology and thermal stability of the microcapsules were tested by Fourier transform infrared spectroscopy, stereo fluorescence microscopy, scanning electron microscopy and thermogravimetric analysis. It was found that the morphology and stability of the new microcapsules prepared by the method are better than those prepared by the traditional complex coacervation method or the in-situ polymerization method. At the same time, it showed that the rotational speed was between 1000 rpm and 1200 rpm, the concentrations of gum arabic and gelatin were 3 wt%, the reaction pH between 3 and 3.5, the reaction duration is between 150 min and 180 min, the ammonium chloride was 20 wt%, and resorcinol was 6 wt%, the reaction between the urea-formaldehyde prepolymer and the electro-neutralizer formed by gelatin and gum arabic was sufficient, the microcapsule wall structure was uniform and consistent, with a dense resin based structure on the outer layer and a flexible blend structure inside. |
关键词 | Gum acacia and gelatin Urea -formaldehyde resin Electrophoresis display microcapsule |
DOI | 10.1016/j.polymer.2024.127205 |
发表期刊 | POLYMER
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ISSN | 0032-3861 |
卷号 | 306页码:11 |
通讯作者 | Cui, Yuehua(yhcui@cigit.ac.cn) |
收录类别 | SCI |
WOS记录号 | WOS:001250038400002 |
语种 | 英语 |